Synthetic Route of 696-07-1, Adding some certain compound to certain chemical reactions, such as: 696-07-1, name is 5-Iodouracil,molecular formula is C4H3IN2O2, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 696-07-1.
5-Iodouracil (23.8 g), TEA (30.3 g), Tol (240 mL) were placed in a 500 mL three-necked flask and heated to 100 C.When the internal temperature of the bottle reached 90 C, phosphorus oxychloride (33.7 g) was slowly added dropwise.After the addition was completed, the temperature was kept stirring for 1 h, then cooled to room temperature, suction filtered, and the filtrate was collected.The solid was washed with PE/EA=5/1, and the filtrate and washing solution were combined.Spin dry to obtain a crude product and then beat with PE to give the product 24.5 g of an off-white solid.The yield was 89%.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 696-07-1, 5-Iodouracil, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Beijing Ruiboao Biological Technology Co., Ltd.; Liu Zhiqiang; Li Yazhou; Chen Zhenchang; Zhang Hongjuan; (7 pag.)CN109761914; (2019); A;,
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