Synthetic Route of 3001-72-7, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 3001-72-7, name is 2,3,4,6,7,8-Hexahydropyrrolo[1,2-a]pyrimidine. This compound has unique chemical properties. The synthetic route is as follows.
N-methyl-1,5-diazabicyclo[4.3.0]non-5-enium dimethyl phosphate ([mDBN][Me2PO4]) was prepared using a Syrris glass-jacketed reactor. For a 250g batch of [mDBN][Me2PO4] the following method was used: 116.89ml (0.946mol) of DBN was charged to the reactor followed by flushing the headspace with argon gas. 110.71ml (0.946mol) of trimethyl phosphate was added to the DBN at 60C under argon atmosphere, as to keep the temperature below 80C during the exothermic reaction. The mixture was then heated to 75C where it was kept for one hour and then cooled to room temperature. The product was an oil-like yellow liquid (Fig. 1).
According to the analysis of related databases, 3001-72-7, the application of this compound in the production field has become more and more popular.
Reference:
Article; Parviainen, Helena; Parviainen, Arno; Virtanen, Tommi; Kilpelaeinen, Ilkka; Ahvenainen, Patrik; Serimaa, Ritva; Groenqvist, Stina; Maloney, Thaddeus; Maunu, Sirkka Liisa; Carbohydrate Polymers; vol. 113; (2014); p. 67 – 76;,
Pyrimidine | C4H4N2 – PubChem,
Pyrimidine – Wikipedia