Related Products of 2915-16-4, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 2915-16-4, name is 2-Chloro-4,6-diphenylpyrimidine. This compound has unique chemical properties. The synthetic route is as follows.
20 g of 11-(3-(dibenzo[b,d]furan-4-yl)phenyl)-11,12-dihydroindole[2,3-a]carbazole,4. A mixture of 8 g of sodium hydride and 300 ml of toluene in a 1 liter flask,And stirred at 40 C under a nitrogen atmosphere. After one hour,Add 12. 8 g of 2-chloro-4,6-diphenyl-1,3-pyrimidine,And continue to stir at 80 C. The reaction was monitored by thin layer chromatography.After completion of the reaction, the reaction mixture was quenched with 200 ml of water,And extracted with 150 ml of ethyl acetate. The organic layer was extracted with 100 ml of water three times and dried over anhydrous sodium sulfate. The collected ethyl acetate layer was further purified by celite column chromatography. The ethyl acetate layer is followed by a rotary evaporatorIn the vacuum was evaporated to dry. The residue was further precipitated by the addition of 100 ml of n-hexane, and 18 g of a yellow solid compound F5 (85% yield) having more than 99% HPLC purity was obtained under vacuum.
According to the analysis of related databases, 2915-16-4, the application of this compound in the production field has become more and more popular.
Reference:
Patent; e-Ray Optoelectronics Technology Co., Ltd; Balaganesan, Banumathy; HUANG, HEH LUNG; KAU, HUANG MING; HSU, PO WEI; (22 pag.)CN106608878; (2017); A;,
Pyrimidine | C4H4N2 – PubChem,
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