Category: 13053-88-8

Adding a certain compound to certain chemical reactions, such as: 13053-88-8, N-(Pyrimidin-2-yl)acetamide, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, COA of Formula: C6H7N3O, blongs to pyrimidines compound. COA of Formula: C6H7N3O

A solution of 2-ampy (0.15 g, 1.59 mmol) in ethanol (10 cm3)was added to a solution of Na2PdCl4 (0.234 g, 0.796 mmol) inmethanol (10 cm3). The mixture was stirred at room temperaturefor 2 h. The yellow solid thus formed was filtered off, washed withmethanol and dried under vacuum 3: Yellow solid, 95%. Anal. Calc. for C12H14N6O2PdCl2: C, 31.9; H,3.1; N, 18.6. Found: C, 32.0; H, 3.4; N, 18.3%. IR: 3267m, 3227m,3078m, 2925m, 1693s, 1517m, 516m, 355m cm1. 1H NMR(DMSO-d6): d 10.55 (s, 2H, NH), 8.63 (d, 1H, pym-H), 7.15 (t, 1H,pym-H), 2.16 (s, 2H, CH3) ppm, 3J(HH) = 4.8 Hz. Melting point:234-236 C.

At the same time, in my other blogs, there are other synthetic methods of this type of compound,13053-88-8, N-(Pyrimidin-2-yl)acetamide, and friends who are interested can also refer to it.

Reference:
Article; Al-Jibori, Subhi A.; Al-Jibori, Qusay K.A.; Schmidt, Harry; Merzweiler, Kurt; Wagner, Christoph; Hogarth, Graeme; Inorganica Chimica Acta; vol. 402; (2013); p. 69 – 74;,
Pyrimidine | C4H4N2 – PubChem,
Pyrimidine – Wikipedia

Reference of 13053-88-8, Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 13053-88-8, name is N-(Pyrimidin-2-yl)acetamide. A new synthetic method of this compound is introduced below.

A solution of 2-acpym (0.0184 g, 0.134 mmol) in CH2Cl2 (5 ml) containing three drops of NEt3 was added to a yellow suspension of 1 (0.0395 g, 0.067 mmol) in CH2Cl2 (10 ml). The yellow solution was stirred for 3 h, filtered and slow evaporation at room temperature gave a yellow precipitate which was recrystallized from CH2Cl2 and MeOH to give a yellow powder (0.041 g, 71%). Anal. Calc. for C17H15ClN4OPd, 47.1, H, 3.5, N, 12.9. Found: C, 47.3, H, 3.4, N, 13.2% IR (KBr) 3330s, 3170s, 3278s, 1649s, 1562s, 460 s cm-1. 1H NMR (dmso-d6) delta 9.42 (d, 1H, J 4.0), 8.66 (d, 1H, J 4.0), 8.57 (s, 1H, NH), 8.47 (s, 1H), 7.84 (dd, 1H, J 7.9, 4.0), 7.67 (d, 1H, J 7.9), 7.47 (d, 1H, J 7.9), 7.19 (dd, 1H, J 4.0, 4.0), 7.13 (dd, 1H, J 7.9, 4.0), 6.97 (dd, 1H, J 7.9, 3.8), 6.78 (dd, 1H, J 4.0, 4.0), 6.31 (d, 1H, J 7.9), 1.63 (s, 3H). Mp 182-184 C.

These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,13053-88-8, its application will become more common.

Reference:
Article; Al-Jibori, Subhi A.; Gergees, Hayfa M.; Al-Rubaye, Mousa S.; Basak-Modi, Sucharita; Ghosh, Shishir; Schmidt, Harry; Laguna, Mariano; Luquin, M. Asuncion; Hogarth, Graeme; Inorganica Chimica Acta; vol. 450; (2016); p. 50 – 56;,
Pyrimidine | C4H4N2 – PubChem,
Pyrimidine – Wikipedia

Electric Literature of 13053-88-8, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 13053-88-8, name is N-(Pyrimidin-2-yl)acetamide. This compound has unique chemical properties. The synthetic route is as follows.

General procedure: For complexes 1-8, a warm solution of ca. two equivalents of ligand (0.151 mmol) in absolute EtOH (10 cm3) was added to a warm solution of [Cd(tsac)2(H2O)] (0.040 g, 0.076 mmol) in absolute EtOH (10 cm3). The mixture was heated to reflux for 3 h. After cooling to room temperature it was filtered and evaporated to half volume. Further slow evaporation of EtOH over several days gave a yellow solid which was collected, washed with absolute EtOH anddried under vacuum

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 13053-88-8, N-(Pyrimidin-2-yl)acetamide.

Reference:
Article; Al-Jibori, Subhi A.; Al-Bayati, Mohamed M.A.; Gergees, Hayfa M.; Wagner, Christoph; Hogarth, Graeme; Inorganica Chimica Acta; vol. 459; (2017); p. 73 – 79;,
Pyrimidine | C4H4N2 – PubChem,
Pyrimidine – Wikipedia