24-Sep News New learning discoveries about 96702-03-3

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 96702-03-3, (S)-2-Methyl-3,4,5,6-tetrahydropyrimidine-4-carboxylic acid, other downstream synthetic routes, hurry up and to see.

Application of 96702-03-3 ,Some common heterocyclic compound, 96702-03-3, molecular formula is C6H10N2O2, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc., below Introduce a new synthetic route.

Example 3 2-Hydroxyethyldimethylammonium 2-methyl-3,4,5,6-tetrahydropyrimidine-4-carboxylate 42.65 g of ectoin are dissolved in 60 ml of water in a 250 ml beaker, and 30 ml of 2-(dimethylamino)ethanol are subsequently added at room temperature with stirring. This reaction solution is stirred at room temperature for a further hour and subsequently evaporated to dryness in a rotary evaporator with a water bath at about 60 C., leaving a white solid.

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 96702-03-3, (S)-2-Methyl-3,4,5,6-tetrahydropyrimidine-4-carboxylic acid, other downstream synthetic routes, hurry up and to see.

Reference:
Patent; MERCK PATENT GESELLSCHAFT; US2011/152292; (2011); A1;,
Pyrimidine | C4H4N2 – PubChem,
Pyrimidine – Wikipedia

24-Sep News New learning discoveries about 96702-03-3

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 96702-03-3, (S)-2-Methyl-3,4,5,6-tetrahydropyrimidine-4-carboxylic acid, other downstream synthetic routes, hurry up and to see.

Application of 96702-03-3 ,Some common heterocyclic compound, 96702-03-3, molecular formula is C6H10N2O2, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc., below Introduce a new synthetic route.

Example 3 2-Hydroxyethyldimethylammonium 2-methyl-3,4,5,6-tetrahydropyrimidine-4-carboxylate 42.65 g of ectoin are dissolved in 60 ml of water in a 250 ml beaker, and 30 ml of 2-(dimethylamino)ethanol are subsequently added at room temperature with stirring. This reaction solution is stirred at room temperature for a further hour and subsequently evaporated to dryness in a rotary evaporator with a water bath at about 60 C., leaving a white solid.

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 96702-03-3, (S)-2-Methyl-3,4,5,6-tetrahydropyrimidine-4-carboxylic acid, other downstream synthetic routes, hurry up and to see.

Reference:
Patent; MERCK PATENT GESELLSCHAFT; US2011/152292; (2011); A1;,
Pyrimidine | C4H4N2 – PubChem,
Pyrimidine – Wikipedia

New downstream synthetic route of 96702-03-3

According to the analysis of related databases, 96702-03-3, the application of this compound in the production field has become more and more popular.

96702-03-3 ,Some common heterocyclic compound, 96702-03-3, molecular formula is C6H10N2O2, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc., below Introduce a new synthetic route.

Example 8 6-Carboxy-2-methyl-1,4,5,6-tetrahydropyrimidinium palmitate 20 g of ectoin are dissolved in 25 ml of water in a 250 ml plastic beaker with magnetic stirrer, and 36.894 g of palmitic acid are subsequently added at room temperature with stirring. This reaction mixture is stirred at room temperature for a further half an hour and subsequently evaporated to dryness in a rotary evaporator with a water bath at about 90 C., leaving a white solid. Melting point 61 C.

According to the analysis of related databases, 96702-03-3, the application of this compound in the production field has become more and more popular.

Reference:
Patent; MERCK PATENT GESELLSCHAFT; US2011/152292; (2011); A1;,
Pyrimidine | C4H4N2 – PubChem,
Pyrimidine – Wikipedia