In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 42487-72-9, name is 2-(Diethylamino)-6-methylpyrimidin-4-ol, the common compound, a new synthetic route is introduced below. Computed Properties of C9H15N3O
In 100ml of dichlorosulfoxide, add 2- (diethylamino) -6-methyl-4-pyrimidinol [2- (diethylamino) -6-methylpyrimidin-4-ol] 18.12g (0.1mol), then 5ml DMF (N, N-dimethylformamide), slowly raise the temperature (1 / min) to 60 , at this temperature, the reaction for 2h. After the reaction was completed, the excess dichlorosulfoxide was distilled off, 100g ice water was added for ultrasonic cleaning for 10 minutes (40KHz), filtered, and the filter cake was dried to constant weight at 80 C to obtain a dark green solid, 4-chloro-N, N-di Ethyl-6-methylpyrimidin-2-amine [4-chloro-N, N-diethyl-6-methylpyrimidin-2-amine].
The synthetic route of 42487-72-9 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Jinhua Shuanghong Chemical Co., Ltd.; Xiao Gang; Xu Jiancheng; (19 pag.)CN110878175; (2020); A;,
Pyrimidine | C4H4N2 – PubChem,
Pyrimidine – Wikipedia