Application of 17180-94-8, In the chemical reaction process,reaction time,type of solvent,can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product.An updated downstream synthesis route of 17180-94-8 as follows.
In a reaction flask, M250g (100mmol), 2-chloro-4,6-diphenyltriazine 20.8g (110mmol), Pd2 (dba) 3 0.9g (0.785mmol, 0.5%), toluene 1500ml, potassium carbonate 43.3 g (314 mmol), reacted at 100 C for 3.5 h. When the reaction is complete, stop the reaction. After cooling to room temperature and filtering, the obtained solid was purified by recrystallization from toluene to obtain white powder A13.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,17180-94-8, its application will become more common.
Reference:
Patent; Beijing Dingcai Technology Co., Ltd.; Xing Qifeng; Zeng Lichang; Li Zhiyang; Huang Xinxin; Gao Yue; (20 pag.)CN110857297; (2020); A;,
Pyrimidine | C4H4N2 – PubChem,
Pyrimidine – Wikipedia