As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 36315-01-2, name is 2-Amino-4,6-dimethoxypyrimidine, molecular formula is C6H9N3O2, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below. 36315-01-2
To the reaction solution ethoxycarbonyl isothiocyanate of 2-amino-4,6-dimethoxy-pyrimidine 124.1g (0.8mol), control the temperature 40 , heat 6h, until starting 2-amino-4, 6- Dimethyloxy completion of the reaction, cooled to room temperature,filtration, and washed with 50mL ethyl acetate to give the product, wet weight of 400g,the product obtained after drying 192.9g, 98.5%, yield 84.3%.
The chemical industry reduces the impact on the environment during synthesis 36315-01-2, I believe this compound will play a more active role in future production and life.
Reference:
Patent; Heilongjiang Kaiao Technology Development Co., Ltd.; GAO, JINSHENG; NIU, LIZHONG; ZUO, DIANFA; LIU, JILONG; MA, YICHAO; (23 pag.)CN105399746; (2016); A;,
Pyrimidine | C4H4N2 – PubChem,
Pyrimidine – Wikipedia