Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 40497-30-1, name is 2-Methylpyrimidine-4,6(1H,5H)-dione. This compound has unique chemical properties. The synthetic route is as follows. Product Details of 40497-30-1
FOX-7 was synthesized according to the method using the procedure of Fu [9]. 2-methylpyrimidine-4,6-dione (2.53 g,0.02 mol) was dissolved in 12mL concentrated H2SO4 (98%), and then 4mL Nitric acid fuming (98%) was dripped in the mixture. The reaction mixture was kept under 15C. After 3 h, the mixture was poured into ice water. The yellow precipitate formed, which was filtered and dried 5 h under vacuum at 50C, yielding 2.40 g (81.1%).The yellow crystal was obtained from C2H5OH solvent. IR (KBr,nu /cm-1): 3407, 3321, 3294, 3216, 1622, 1501, 1473, 1388, 1328, 1201,1161, 1133, 1020, 620, 453 cm-1.
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Reference:
Article; Li, Keyao; Ren, Xiangwen; Fu, Shuqin; Zhu, Jiaping; Journal of Molecular Structure; vol. 1173; (2018); p. 26 – 32;,
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