Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 52854-14-5, name is 4-Chloro-6-methoxy-5-nitropyrimidine. A new synthetic method of this compound is introduced below., COA of Formula: C5H4ClN3O3
Example 12 4-methoxy-6-dimethyldithiocarbamoyl-5-nitropyrimidine (14) A solution of 4-methoxy-6-chloro-5-nitropyrimidine (0.5 g, 2.6 mmol), sodium dimethyldithiocarbamate dihydrate (0.6 g, 3.3 mmol) and ethanol (40 mL) was mixed for 1 hour at room temperature. Reaction mixture was diluted by water (80 mL), light yellow solid was filtered and purified by crystallization from methanol to give 0.4 g of pure title compound as an bright yellow crystalline solid, m.p. 122-125ØC.
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Reference:
Patent; MEDAC GmbH; EP1312607; (2003); A1;,
Pyrimidine | C4H4N2 – PubChem,
Pyrimidine – Wikipedia