Related Products of 857641-46-4, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 857641-46-4, name is 2-(4-Bromo-1H-pyrazol-1-yl)pyrimidine, molecular formula is C7H5BrN4, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
General procedure: The ligand pzpm (47.4mg, 0.32mmol) was dissolved in CH2Cl2 (10ml), and added to a suspension of [NiBr2(DME)] (100mg, 0.32mmol) in CH2Cl2 (20ml), in a Schlenk tube, under nitrogen. The reaction was stirred for 18h at room temperature. The resulting suspension was filtered and the solid product was washed twice with hexane (2×10ml) and dried in vacuum, yielding 94mg (82%) of a mustard yellow powder.
According to the analysis of related databases, 857641-46-4, the application of this compound in the production field has become more and more popular.
Reference:
Article; Moreno-Lara, Belen; Carabineiro, Sonia A.; Krishnamoorthy, Paramasivam; Rodriguez, Ana M.; Mano, Joao F.; Manzano, Blanca R.; Jalon, Felix A.; Gomes, Pedro T.; Journal of Organometallic Chemistry; vol. 799-800; (2015); p. 90 – 98;,
Pyrimidine | C4H4N2 – PubChem,
Pyrimidine – Wikipedia