Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 6328-58-1, name is 6-Methyl-2-(methylthio)-1H-pyrimidin-4-one. This compound has unique chemical properties. The synthetic route is as follows. name: 6-Methyl-2-(methylthio)-1H-pyrimidin-4-one
A mixture of the pyrimidone (324b; 437g), iodine (852.6g) and sodium hydroxide (134.2g) in water (2L) was heated to 80C for 15h. After cooling the reaction was neutralized with acetic acid and the solid collected to give the iodide (324c; 656g) as a light-brown solid. Used in the next step without purification.
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Reference:
Patent; SCHERING CORPORATION; SOUTHERN RESEARCH INSTITUTE; ARASAPPAN, Ashok; NJOROGE, F., George; BENNETT, Frank; GIRIJAVALLABHAN, Vinay, M.; HUANG, Yuhua; HUELGAS, Regina; PIWINSKI, John, J.; SHIH, Neng-Yang; VERMA, Vishal; VELAZQUEZ, Francisco; VENKATRAMAN, Srikanth; KWONG, Cecil, D.; ANANTHAN, Subramaniam; CLARK, Jeremy; GENG, Feng; KEZAR, Hollis, S., III.; MADDRY, Joseph, A.; REYNOLDS, Robert, C.; ROYCHOWDHURY, Abhijit; SECRIST, John, A., III.; FOWLER, Anita, T.; WO2010/22121; (2010); A1;,
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