Related Products of 89284-85-5, Adding some certain compound to certain chemical reactions, such as: 89284-85-5, name is Methyl 2,5,6-trichloropyrimidine-4-carboxylate,molecular formula is C6H3Cl3N2O2, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 89284-85-5.
Furfurylamine (0.155 g, 1.60 mmol) was added to a stirred solution of 6- methoxycarbonyl-2,4,5-trichloropyrimidine (prepared as described in example 4) (0.193 g, 0.80 mmol) and triethylamine (0.24 ml, 1.7 mmol) in dichloromethane (3 ml). The solution was stirred at ambient temperature for 18 hours, and then added to a mixture of ethyl acetate and brine. The organic phase was dried over magnesium sulphate, filtered and evaporated under reduced pressure to give an orange solid. This was purified by column chromatography on silica using ethyl acetate:hexane (1 :2) as eluent to provide 2,5-dichloro-4-(furan-2-ylmethylamino)-6-methoxycarbonylpyrimidine as a pale yellow solid (0.195 g, 81 %). Characterising data for this compound are as follows: m.p. 110- 112 0C; 1H nmr (400 MHz, CDCI3) deltaH 7.40 (1H, m), 6.35 (2H, m), 6.16 (1H, br s), 4.72 (2H, d), 3.98 (3H, s) ppm.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 89284-85-5, Methyl 2,5,6-trichloropyrimidine-4-carboxylate, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; SYNGENTA LIMITED; WO2009/81112; (2009); A2;,
Pyrimidine | C4H4N2 – PubChem,
Pyrimidine – Wikipedia